I agree on the use of Norman Koren's charts. They will help you evaluate the critical resolution at 10% and 50% MTF, not just minimum discernible resolution. You can print as many as you need and arrange them however you want (and I agree to put one at a 45-degree angle--very important).
Koren's article on lens testing, but it applies here
His chart can be downloaded and printed. I would use matte-surface paper. Include a big black square on the same print. Also, include a known-good gray card somewhere in the image for calibrating any needed color corrections.
Make sure your film exposures are perfect. That means confirming the shutter, or bracketing if you aren't sure.
Rick "who has done this with medium-format, and used a microscope for evaluation" Denney
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