PDA

View Full Version : Unusual grain pattern, like styrofoam or brains?



nathanm
30-Aug-2011, 11:32
I'm wondering what might be going on here with the grain. The film is Tri-X, developer is Ilford Perceptol, I'm guessing the temperature was about 75ºF. plain water stop bath, old-ish jug of Photographer's Formulary TF4 fixer. Constant agitation in BTZS tubes for about 8 minutes. It's not a huge bummer, (although it would be a real interesting challenge to try and get rid of it!) I've just never seen this particular grain effect before and was curious about what might have caused it. Maybe it's really common and I'm just a newb. Entirely possible. Anyway, thanks!

http://nathanmarciniak.com/pix/clumpygrain.jpg

Ari
30-Aug-2011, 11:46
This looks like reticulation to me, but more knowledgeable people may differ.
This happens when you go from a high temperature to a low temperature; the emulsion expands and contracts rapidly, or "crinkles".
If your developer was 75˚F, you might want to double-check the temperature of your other baths when you last used them.
Odds are, the fixer, stop bath, or wash water were at a much lower temperature than your developer.

E. von Hoegh
30-Aug-2011, 11:49
+1 on reticulation and the causes. You shouldn't be guessing at temperature. Thermometers are cheap these days.:)

nathanm
30-Aug-2011, 11:59
I did measure the temperature of the developer, but guessing about what the number was now. It seems odd that it would be different than the other chemicals, but maybe it was.

al olson
30-Aug-2011, 12:14
I agree. Was your water stop bath fresh from the spigot? If so, check the temperature of your cold water line. Going from 75 degrees to a water temp of 60 or 65 might be the cause of your problem.

lenser
30-Aug-2011, 12:29
Definitely looks exactly like the retriculation I've experienced. Always caused by a big temp difference with hot developer and considerably colder stop bath or water if you use that for a stop before fixing. Simply put, the emulsion is softened by a too warm developer and then shocked and shrunk rapidly by the colder stop or water and everything separates and draws up into these little "islands" of the emulsion.

Now I am very sure to keep temps within a few degrees of each other all the way through the wash cycle.

Jay DeFehr
30-Aug-2011, 12:35
Reticulation due to extreme temperature differential. I think we've all done it once.

Sevo
30-Aug-2011, 13:29
Congratulations, this is genuine reticulation. People often fail to get there when trying to do it as an effect...

It is not easy to arrive there at a constant 75°F. If there hasn't been some step in the process whose temperature was way off (tap water always is a danger, in either direction), another common cause is accidentally using the bottle with concentrate in place of the diluted stop - pH difference shocks may also cause reticulation.

nathanm
30-Aug-2011, 13:47
Oh well, then um, yeah I was trying to achieve this reticulation effect! A photographic achievement on my part for sure! Hooray me! :p

No, but seriously - thanks for all the replies! I will have to be more careful with the temps next time.

Jim Jones
30-Aug-2011, 14:03
I keep film tanks and trays, chemicals. and an adequate supply of water for washhing in the darkroom so all are about the same temperature. When develping in trays there will be a change in temperature due to evaporation, but it hasn't caused noticable problems yet.

nathanm
30-Aug-2011, 14:34
That's a good idea Jim. In my case it was probably was the wash water that was the temperature variable, everything else was just sitting in bottles in the room.

Robert Hughes
30-Aug-2011, 15:07
In its most severe form, that temperature differential can cause emulsion to lift right off the backing. Quite a bit of the newsreel film of the Allied invasion of Normandy on June 6,1944 was ruined by an overenthusiastic lab tech who ran his developer bath too hot. Talk about no chance for a second take!

tbeaman
30-Aug-2011, 15:11
Yikes, that's a big "ouch" for history!

Interesting, this is the first time I'm seeing the fabled reticulation effect. Not because I'm some processing guru, I just have very little experience doing black and white. Anyway, I can see why some go for it. It looks like an aged painting.

BetterSense
30-Aug-2011, 15:29
That looks exactly like the reticulation I got with Neopan 400. I found that film, or that batch of it, particularly prone to it. I think I blamed it on leaving my running water wash going and the water temperature changing drastically as usage in my apartment changed.